Pengaruh Suhu Ekstraksi dan Kecepatan Pengadukan terhadap Karakteristik Crude Ekstrak Stevia
DOI:
https://doi.org/10.32734/jtk.v13i2.17131Keywords:
crude stevia extract, maceration, stevia, stirring speed, temperatureAbstract
Stevia is a natural sweetener that is 250-300 times sweeter than sucrose and is low in calories. Stevia sweeteners are obtained from the extraction of stevia leaves. This study aims to determine the effects of temperature and stirring speed on the characteristics of crude stevia extract (yield, brix value, and IR spectrum). Maceration extraction was conducted with 70% ethanol for 1 hour, varying the temperature (28 ℃, 40 ℃, 55 ℃) and stirring speed (0 rpm, 50 rpm, 100 rpm, 150 rpm). The results showed that a temperature of 40 ℃ produced the highest yield at each stirring speed. The yield increased with the increase in stirring speed at each extraction temperature. The highest brix value was obtained at 55 ℃ and a stirring speed of 150 rpm. The IR spectrum results showed that the functional groups in the crude stevia extract were almost identical to those in commercial stevia.
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References
BPS, “Distribusi Perdagangan Komoditas Gula Pasir,†Jakarta, 2021. [Online]. Available: https://www.bps.go.id/id/publication/2021/10/29/dd4ff6a48b14ca26d492ed73/distribusi-perdagangan-komoditas-gula-pasir-indonesia-2021.html.
S. Meylinah, “Indonesia: Sugar Annual,†Jakarta, 2021. [Online]. Available: https://www.fas.usda.gov/data/indonesia-sugar-annual-5.
AGI, “National Sugar Summit 2020,†2020. https://asosiasigulaindonesia.org/wp-content/uploads/2020/11/Proposal_Indo1-2.pdf (accessed Sep. 21, 2024).
R. Castro-Muñoz et al., “Natural sweeteners: Sources, extraction and current uses in foods and food industries,†Food Chem., vol. 370, no. 130991, pp. 1–18, 2022, doi: 10.1016/j.foodchem.2021.130991.
N. A. Neacşu and A. Madar, “Artifical Sweeteners Versus Natural Sweeteners,†Bull. Transilv. Univ. Braşov Ser. V Econ. Sci., vol. 7 (56), no. 1, pp. 59–64, 2014.
P. Singh, Y. G. Ban, L. Kashyap, A. Siraree, and J. Singh, “Sugar and Sugar Substitutes: Recent Developments and Future Prospects,†in Mohan, N., Singh, P. (eds) Sugar and Sugar Derivatives: Changing Consumer Preferences, Singapore: Springer, 2020, pp. 39–75.
M. C. Carakostas, L. L. Curry, A. C. Boileau, and D. J. Brusick, “Overview: The history, technical function and safety of rebaudioside A, a naturally occurring steviol glycoside, for use in food and beverages,†Food Chem. Toxicol., vol. 46, no. 7, pp. 1–10, 2008, doi: 10.1016/j.fct.2008.05.003.
M. Dyduch-Siemińska, A. Najda, J. Gawroński, S. Balant, K. Świca, and A. Żaba, “Stevia rebaudiana Bertoni, a source of high-potency natural sweetener—biochemical and genetic characterization,†Molecules, vol. 25, no. 4: 767, pp. 1–12, 2020, doi: 10.3390/molecules25040767.
M. Yildiz and M. Karhan, “Characteristics of some beverages adjusted with stevia extract, and persistence of steviol glycosides in the mouth after consumption,†Int. J. Gastron. Food Sci., vol. 24, no. 100326, pp. 1–8, Jul. 2021, doi: 10.1016/j.ijgfs.2021.100326.
Djajadi, “Pengembangan Tanaman Pemanis Stevia rebaudiana (Bertoni) di Indonesia,†Perspekt. Rev. Penelit. Tanam. Ind., vol. 13, no. 1, pp. 25–33, 2014, doi: 10.21082/p.v13n1.2014.%p.
A. Marlina and E. Widiastuti, “Pembuatan Gula Cair Rendah Kalori Dari Daun Stevia Rebaudiana Bertoni Secara Ekstraksi Padat-Cair,†in 9th Industrial Research Workshop and National Seminar, 2018, pp. 149–154, [Online]. Available: https://jurnal.polban.ac.id/ojs-3.1.2/proceeding/article/view/1062/864.
E. M. Nahor, B. I. Rumagit, and H. Y. Tou, “Comparison of the Yield of Andong Leaf Ethanol Extract (Cordyline fruticosa L.) Using Maceration and Sokhletation Extraction Methods,†in Seminar Nasional 2022 Interprofessional Collaboration dalam Pengembangan Center of Excellence Inovasi Bahan Lokal pada Era New Normal, 2020, vol. 1, no. 1, pp. 40–44, [Online]. Available: https://ejurnal.poltekkes-manado.ac.id/index.php/prosiding2020/issue/view/125.
M. Shachman, The Soft Drinks Companion: A Technical Handbook for the Beverage Industry. Boca Raton: CRC Press Taylor & Francis Group, 2004.
N. Faradillah, A. Hintono, and Y. B. Pramono, “Karakteristik Permen Karamel Susu Rendah Kalori Dengan Proporsi Sukrosa Dan Gula Stevia (Stevia Rebaudiana) Yang Berbeda,†J. Apl. Teknol. Pangan, vol. 6, no. 1, pp. 39–42, 2017, doi: 10.17728/jatp.206.
J. F. Richardson, J. H. Harker, and J. R. Backhurst, “Chemical Engineering Volume 2: Particle Technology and Separation Processes,†in Chemical Engineering Series, 5th Ed., vol. 2, Amsterdam, The Netherlands: Elsevier, 2002, pp. 721–770.
Ani Purwanti, M. Yusuf, W. Prayogo, and U. A. Ambarita, “Penentuan Koefisien Transfer Massa Padat Cair Pada Sistem Tawas Air Dengan Variasi Kecepatan Putaran Dan Diameter Pengaduk,†KURVATEK, vol. 7, no. 1, pp. 63–70, 2022, doi: 10.33579/krvtk.v7i1.3128.
M. Qibtiyah, “Pengaruh Variasi Suhu dan Waktu Ekstraksi Metode Maserasi Dinamik (Water-Bath Shaker) Terhadap Rendemen Ekstrak dan Aktivitas Antioksidan Ekstrak Daun Stevia rebaudiana Bert. M,†Universitas Islam Negeri Syarif Hidayatullah, 2019.
A. N. A. Zain and B. Nurhadi, “Pengaruh Penambahan Rasio Bahan Pengikat Terhadap Aktivitas Antioksidan Bubuk Stevia (Stevia Rebaudiana Bertoni),†in Prosiding Seminar Nasional Agribisnis, 2020, no. 1, pp. 32–37, [Online]. Available: https://ejournal.unkhair.ac.id/index.php/semnasagribisnis/article/view/2440.
H. Hasnaeni, S. Usman, and W. Wisdawati, “Pengaruh Metode Ekstraksi Terhadap Rendemen Dan Kadar Fenolik Ekstrak Tanaman Kayu Beta-Beta (Lunasia amara Blanco),†J. Farm. Galen. (Galenika J. Pharmacy), vol. 5, no. 2, pp. 175–182, 2019, doi: 10.22487/j24428744.2019.v5.i2.13599.
S. Vasquez and S. Mueller, “Refractometer calibration , use and maintenance,†University of California Cooperative Extension Fresno County, 2001. https://iv.ucdavis.edu/files/24488.pdf (accessed Sep. 21, 2024).
C. R. Utami, “Pengaruh Waktu Fermentasi Terhadap Karaktersitik Kimia Dan Organoleptik Tape Pisang Kepok,†Teknol. Pangan Media Inf. dan Komun. Ilm. Teknol. Pertan., vol. 8, no. 1, pp. 99–106, 2017, doi: 10.35891/tp.v8i1.904.
Q. W. Zhang, L. G. Lin, and W. C. Ye, “Techniques for extraction and isolation of natural products: A comprehensive review,†Chin. Med., vol. 13, no. 1, pp. 1–26, 2018, doi: 10.1186/s13020-018-0177-x.
S. Martono, Y., Riyanto, S., Rohman, A., & Martono, “Optimum ultrasound extraction of stevioside and rebaudioside a from Stevia rebaudiana leaves on isocratic RP-HPLC analysis,†in Proceedings of the International Conference on Science and Science Education, 2015, pp. 149–155.
R. Chang and K. Goldsby, Chemistry, 12th ed. New York: McGraw Hill Education, 2015.
L. S. Celaya, E. Kolb, and N. Kolb, “Solubility of Stevioside and Rebaudioside A in water, ethanol and their binary mixtures,†Int. J. Food Stud., vol. 5, no. 2, pp. 158–166, 2016, doi: 10.7455/ijfs/5.2.2016.a4.
Indah Cikita, Ika Herawati Hasibuan, and Rosdanelli Hasibuan, “Pemanfaatan Flavonoid Ekstrak Daun Katuk (Sauropus Androgynus (L) Merr) Sebagai Antioksidan Pada Minyak Kelapa,†J. Tek. Kim. USU, vol. 5, no. 1, pp. 45–51, 2016, doi: 10.32734/jtk.v5i1.1524.
D. Maulida and N. Zulkarnaen, “Ekstraksi Antioksidan (Likopen) dari Buah Tomat dengan Menggunakan Solven Campuran, N – Heksana, Aseton, dan Etanol,†UNDIP Website, Semarang, 2010. [Online]. Available: http://eprints.undip.ac.id/13444/.
S. Margaretta, S. D. Handayani, N. Indraswati, and H. Hindarso, “Ekstraksi Senyawa Phenolic Pandanus Amaryllifolius Roxb. sebagai Antioksidan Alami,†Widya Tek., vol. 10, no. 1, pp. 21–30, 2013, doi: 10.33508/WT.V10I1.157.
C. J. Geankoplis, Transport Processes and Unit Operations, 3rd ed. New Jersey: PTR Prentice Hall, 1993.
F. S. Budi and S. B. Sasongko, “Koefisien Transfer Massa pada Proses Ekstraksi Kayu Manis (Cinnamomum Burmanni),†Reaktor, vol. 12, no. 4, pp. 232–238, 2009, doi: https://doi.org/10.14710/reaktor.12.4.232 – 238.
D. Naviglio, F. Pizzolongo, L. Ferrara, B. Naviglio, A. Aragòn, and A. Santini, “Extraction of pure lycopene from industrial tomato waste in water using the extractor Naviglio ®,†African J. Food Sci., vol. 2, no. 2, pp. 37–44, 2008.
J. M. Prado and M. A. Rostagno, Natural Product Extraction: Principles and Applications. Cambridge: The Royal Society of Chemistry, 2013.
M. Plaza and C. Turner, “Pressurized hot water extraction of bioactives,†Trends Anal. Chem., vol. 71, pp. 39–54, 2015, doi: 10.1016/j.trac.2015.02.022.
P. Panja and M. Mukhopadhyay, “Extraction of Natural Sweetener from Stevia Leaves Using Pressurized Hot Water,†J. Nutraceuticals Food Sci., vol. 4, no. 13, pp. 1–9, 2019.
D. Dachriyanus, Analisis Struktur Senyawa Organik secara Spektroskopi. Padang: Lembaga Pengembangan Teknologi Informasi dan Komunikasi (LPTIK) Universitas Andalas, 2017.
D. A. Skoog, F. J. Holler, and S. R. Crouch, Principles of Instrumental Analysis, 6th Ed. Pacific Grove: Thomson Brooks/Cole, 2007.
J. A. Considine and E. Frankish, A Complete Guide to Quality in Small-Scale Wine Making. Amsterdam, The Netherlands: Elsevier, 2014.
J. Moore, “Steviol Glycosides: Chemical and Technical Assessment ( CTA ),†Food and Agriculture Organization of the United Nations, 2017. https://openknowledge.fao.org/server/api/core/bitstreams/38aa454a-e164-4f3e-95c0-bb4938d8aa90/content (accessed Sep. 21, 2024).
A. Abubakar and M. Haque, “Preparation of medicinal plants: Basic extraction and fractionation procedures for experimental purposes,†J. Pharm. Bioallied Sci., vol. 12, no. 1, pp. 1–10, 2020, doi: 10.4103/jpbs.JPBS_175_19.
BSN, “SNI 3140.3:2010 Gula Kristal - Bagian 3 : Putih,†2010. [Online]. Available: http://sispk.bsn.go.id/SNI/DetailSNI/7783.
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