Penyediaan Biofilm Berbasis Pektin Kulit Buah Cempedak (Artocarpus champaden L.) Terisi Carboxymethyl Cellulose dengan Variasi Konsentrasi Gliserol Untuk Menurunkan Susut Bobot Buah Mangga
DOI:
https://doi.org/10.32734/jtk.v14i1.18721Keywords:
cempedak, pectin, biofilm, glycerol, mangoAbstract
Cempedak peel contains 38.85% pectin compounds and has the potential to become biofilm raw material. The characteristics of pectin-based biofilm can be improved by the addition of a glycerol plasticizer. This study aims to determine the effect of variations in glycerol concentration (0%; 3%; 5%; 7% and 9%) on biofilm charactersitics and biofilm application on the shelf life of mango fruit. Pectin was extracted using 5% citric acid at 85°C or 90 minutes. Biofilms were applied on mango fruit for 8 days. Analysis of pectin compounds showed a yield 22.09%; ash content 7.40%; equivalent weight 588.235 mg; methoxyl content 6.20%; galacturonic acid content 36.12%. Analysis of physical properties and biofilm application on mango fruit showed a density value of 2.833 g/mL; water solubility 79.41%; mango weight loss of 33.47%; and a deacrease in vitamin C of 5%. SEM-EDX analysis showed the pectin particles were homogeneous fine grains and dominated by the element of oxygen (O) 88.84%. FTIR analysis of cempedak fruit peel pectin and biofilm showed functional groups of O-H; C-H (methyl); C=O; C-O; C-C.
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References
D. N. A. Dahlan, “Perbandingan kandungan serat kasar selai cempedak yang diperam secara tradisional dan menggunakan karbid,” J. Biol. Educ., vol. 3, no. 1, pp. 63–71, 2020.
Nurhaeni, N. A. Tjiang, J. Hardi, Diharnaini, and Khairunnisa, “Ekstraksi dan karakterisasi pektin dari kulit dan dami buah cempedak (Artocarpus chempeden),” KOVALEN, vol. 4, no. 3, pp. 304–315, 2018.
Badan Pusat Statistik, “Produksi Tanaman Buah-Buahan, 2021-2023,” bps.go.id, 2024. https://www.bps.go.id/id/statistics-table/2/NjIjMg==/produksi-tanaman-buah-buahan.html (accessed Jul. 12, 2024).
J. P. Maran and B. Priya, “Ultrasound-assisted extraction of pectin from sisal waste,” Carbohydr. Polym., vol. 115, no. 1, pp. 732–738, 2014.
A. Arimpi and S. Pandia, “Pembuatan pektin dari limbah kulit jeruk (Citrus sinensis) dengan metode ekstraksi gelombang ultrasonik menggunakan pelarut asam sulfat (H2SO4),” J. Tek. Kim. USU, vol. 8, no. 1, pp. 18–24, 2019.
Y. Darni, H. Utami, R. Septiana, and R. A. Fitriana, “Comparative studies of the edible film based on low pectin methoxyl with glycerol and sorbitol plasticizers,” J. Bahan Alam Terbarukan, vol. 6, no. 2, pp. 158–167, 2017.
T. M. P. Ngo, T. H. Nguyen, T. M. Q. Dang, T. V. T. Do, A. Reungsang, N. Chaiwong, and P. Rachtanapun, “Effect of pectin/nanochitosan-based coatings and storage temperature on shelf-life extension of “elephant” mango (Mangifera indica L.) fruit,” Polymers, vol. 13, no. 3430, pp. 1–22, 2021.
V. G. Poosarla, S. Bisoi, A. Siripurapu, B. G. Rathod, A. Ramadoss, S. Kilaprthi, N. Shivshetty, and G. Rajagopalan, “Extension of shelf life of tomato (Solanum lycopersicum L.) by using a coating of polyhydroxybutyrate-carboxymethyl cellulose-pectin-thymol conjugate,” J. Food Sci., vol. 89, no. 2024, pp. 6232–6252, 2024.
T. M. P. Ngo, T. H. Nguyen, T. M. Q. Dang, T. X. Tran, and P. Rachtanapun, “Characteristics and antimicrobial properties of active edible films based on pectin and nanochitosan,” Int. J. Mol. Sci., vol. 21, no. 6, pp. 1–16, 2020.
I. G. Moorthy, J. P. Maran, S. Ilakya, S. L. Anitha, S. P. Sabarima, and B. Priya, “Ultrasound assisted extraction of pectin from waste Artocarpus heterophyllus fruit peel,” Ultrason. Sonochem., vol. 34, pp. 525–530, 2017.
R. Suhag, N. Kumar, A. T. Petkoska, and A. Upadhyay, “Film formation and deposition methods of edible coating on food products: a review,” Food Res. Int., vol. 136, no. 2020, pp. 1–16, 2020.
M. Moalemiyan, H. S. Ramaswamy, and N. Maftoonazad, “Pectin-based edible coating for shelf-life extension of Ataulfo mango,” J. Food Process Eng., vol. 35, no. 4, pp. 1–29, 2011.
T. Karbowiak, H. Hervet, L. Léger, D. Champion, F. Debeaufort, and A. Voilley, “Effect of plasticizers (water and glycerol) on the diffusion of a small molecule in iota-carrageenan biopolymer films for edible coating application,” Biomacromolecules, vol. 7, no. 6, pp. 2011–2019, 2006.
P. Picauly and G. Tetelepta, “Pengaruh konsentrasi gliserol pada edible coating terhadap perubahan mutu buah pisang tongka langit (Musa troglodytarium L.) selama penyimpanan,” AGRITEKNO, vol. 7, no. 1, pp. 16–20, 2018.
S. Panahirad, M. Dadpour, S. H. Peighambardoust, M. Soltanzadeh, B. Gullon, K. Alirezalu, and J. M. Lorenzo, “Applications of carboxymethyl cellulose- and pectin-based active edible coatings in preservation of fruits and vegetables: A review,” Trends Food Sci. Technol., vol. 110, no. 2021, pp. 663–673, 2021.
M. S. Rahman, M. S. Hasan, A. S. Nitai, S. Nam, A. K. Karmakar, M. S. Ahsan, M. J. A. Shiddiky, and M. B. Ahmed, “Recent developments of carboxymethyl cellulose,” Polymers, vol. 13, no. 1345, pp. 1–48, 2021.
P. Wisudawaty, I. Yuliasih, and L. Haditjarako, “Pengaruh edible coating terhadap kapasitas air terikat sekunder dan tersier manisan tomat cherry selama penyimpanan,” J. Teknol. Ind. Pertan., vol. 26, no. 3, pp. 301–310, 2016.
S. Roikah, W. D. P. Rengga, Latifah, and E. Kusumastuti, “Ekstraksi dan karakterisasi pektin dari belimbing wuluh (Averrhoa bilimbi L),” J. Bahan Alam Terbarukan, vol. 5, no. 1, pp. 29–36, 2016.
I. K. Dewi, N. Khoirina, and N. A. C. Imani, “Pengaruh variasi konsentrasi gliserol pada edible coating dari ekstraksi pektin limbah kulit durian sebagai pengawet pada cabai rawit merah untuk memperpanjang massa simpan,” Kejuangan, pp. 1–6, 2020.
A. Adhiksana, “Perbandingan metode konvensial ekstraksi pektin dari kulit buah pisang dengan metode ultrasonik,” J. Res. Technol., vol. 3, no. 2, pp. 80–88, 2017.
S. Ranganna, Handbook of Analysis and Quality Control for Fruit and Vegetable Products, 2nd ed. New Delhi: Tata McGraw-Hill, 2000.
A. Tuhuloula, L. Budiyarti, and E. N. Fitriana, “Karakterisasi pektin dengan memanfaatkan limbah kulit pisang menggunakan metode ekstraksi,” Konversi, vol. 2, no. 1, pp. 21–27, 2013.
H. Widodo, E. Kustiyah, N. W. Sari, Andhy, and M. Prastia, “Ekstraksi pektin dari kulit pisang dengan proses sokletasi,” J. Siliwangi, vol. 5, no. 1, pp. 28–31, 2019.
E. P. D. Saputra and H. Saputra, “Karakterisasi plastik biodegredable dari pati limbah kulit pisang muli dengan plasticizer sorbitol,” J. Teknol. Pertan. Andalas, vol. 24, no. 1, pp. 29–36, 2014.
S. S. Udjiana, S. Hadiantoro, A. Takwanto, and A. W. Mustikarini, “Peningkatan karakteristik biodegredable plastics dari kuit pisang candi dengan penambahan filler kalsium silikat clay,” J. Tek. Kim. dan Lingkung., vol. 4, no. 2, pp. 175–185, 2020.
M. T. Iglesias and J. E. Lozano, “Extraction and characterization of sunflower pectin,” J. Food Eng., vol. 62, no. 3, pp. 215–223, 2004.
T. H. McHugh and J. M. Krochta, “Sorbitol-vs-glycerol-plasticized whey protein edible films: integrated oxygen permeability and tensile property evaluation,” J. Agric. Food Chem., vol. 39, no. 11, pp. 841–845, 1994.
D. L. Pavia, G. M. Lampman, G. S. Kriz, and J. R. Vyvyan, Introduction to Spectroscopy, 5th ed. 2013.
A. B. D. Nandiyanto, R. Oktiani, and R. Ragadhita, “How to read and interpret ftir spectroscope of organic material,” Indones. J. Sci. Technol., vol. 4, no. 1, pp. 97–118, 2019.
H. Sastrohamidjojo, Dasar-Dasar Spektroskopi. Yogyakarta: Gajah Mada University Press, 2018.
S. A. Yudistirani, Susanty, R. D. U., and H. N., “Pengaruh variasi konsentrasi gliserol dari minyak jelantah terhadap nilai uji tarik bioplastik dari pemanfaatan limbah kulit ari kacang kedelai,” KONVERSI, vol. 8, no. 1, pp. 55–60, 2019.
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